N,N-Dimethyl-5-nitropyridin-2-amine

N,N-Dimethyl-5-nitropyridin-2-amine³⁰ (3d)

Yellow solid; mp 155-157 °C; 

¹H NMR (DMSO-d₆, 400 MHz) 

δ 9.02 (d, 1H, J 2.8 Hz), 

8.26 (dd, 1H, J 9.2; 2.8 Hz), 

6.80 (d, 1H, J 9.2 Hz), 

3.25 (s, 6H); 

IR (KBr) ν_max/cm^-1: 2924, 2854, 1597, 1335, 1295, 1118, 810; 

MS (CI method): 168 (M+1, 100%).

30. Heindel, N. D.; Kannewell, P. D.; Chem. Commun. 1969, 38.         [ Links ]