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Friday, 22 January 2016

1-(4-bromo-1H-pyrrol-2-yl)-2,2,2-trichloroethanone



1-(4-Bromo-1H-pyrrol-2-yl)-2,2,2-trichloroethanone
 72652-32-5



(mp 140–143 °C):

1H NMR (400 MHz, DMSO-d6
δ 12.84 (br s, 1H),
7.53 (br s, 1H),
7.31 (s, 1H);  



13C NMR (100 MHz, DMSO-d6)
δ 171.6, c=o
129.0, c-c=o
122.0, NH CH
121.5,
97.5, CBr
94.5; CCl3


HRMS-ESI (m/z) calcd for C6H2BrCl3NO [M – H] 287.8380 and 289.8365, found 287.8374 and 289.8346




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O=C(c1cc(Br)c[nH]1)C(Cl)(Cl)Cl




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Taiz
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Taiz is a city in the Yemeni Highlands, near the famous Mocha port on the Red Sea, lying at an elevation of about 1,400 metres above sea level and Sabir Mountain that neighbors it rises the 3,006 metres above the city. Wikipedia

 

 
 

 
 

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