Methyl 5-(2,2-Dimethoxyethylcarbamoyl)-3-(benzyloxy)-1,4-dihydro-1-(2,2-dimethoxyethyl)-4-oxopyridine-2-carboxylate

Methyl 5-(2,2-Dimethoxyethylcarbamoyl)-3-(benzyloxy)-1,4-dihydro-1-(2,2-dimethoxyethyl)-4-oxopyridine-2-carboxylate (imp-2)

1H NMR (400 MHz, CDCl3) δ 10.1 (t, J = 5.2 Hz, 1H), 8.4 (s, 1H), 7.3–7.4 (m, 5H), 5.2 (s, 2H), 4.5(t, J = 5.2 Hz, 1H), 4.4 (t, J = 4.4 Hz, 1H), 4.0 (d, J = 4.4hz, 2H), 3.7 (s, 3H), 3.6 (t, J = 6.0 Hz, 2H), 3.4 (s, 6H), 3.3 (s, 6H) ; 

13C NMR (400 MHz, CDCl3) δ 173.2, 164.2, 162.1, 148.2, 144.4, 136.7, 134.8, 128.5, 128.3, 128.1, 119.3, 102.7, 102.4, 74.3, 56.8, 55.6, 53.9, 53.1, 40.8;

 IR (KBr, cm–1): 3201, 3045, 2949, 2835, 1734, 1662, 1610, 1548;

 ESI-MS m/z 479.26.

http://pubs.acs.org/doi/suppl/10.1021/acs.oprd.6b00156/suppl_file/op6b00156_si_001.pdf

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SIDON, LEBANON

Sidon

City in Lebanon

Sidon or Saïda is the third-largest city in Lebanon. It is located in the South Governorate of Lebanon, on the Mediterranean coast, about 40 kilometres north of Tyre and 40 km south of the capital, Beirut. Wikipedia

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