DR ANTHONY MELVIN CRASTO,WorldDrugTracker, helping millions, A 90 % paralysed man in action for you, I am suffering from transverse mylitis and bound to a wheel chair, With death on the horizon, nothing will not stop me except God................DR ANTHONY MELVIN CRASTO Ph.D ( ICT, Mumbai) , INDIA 25Yrs Exp. in the feld of Organic Chemistry,Working for GLENMARK GENERICS at Navi Mumbai, INDIA. Serving chemists around the world. Helping them with websites on Chemistry.Million hits on google, world acclamation from industry, academia, drug authorities for websites, blogs and educational contribution
Showing posts with label ALIBAG. Show all posts
Showing posts with label ALIBAG. Show all posts

Tuesday 7 July 2015

1-Aminomethylcyclopropanecarboxylic acid ethyl ester





1-Aminomethylcyclopropanecarboxylic acid ethyl ester


1=http://orgspectroscopyint.blogspot.in/2015/07/1-cyanocyclopropanecarboxylic-acid.html

 
1-Cyanocyclopropanecarboxylic acid ethyl ester

To a stirred solution of compound 1
1-Cyanocyclopropanecarboxylic acid ethyl ester(2.35 g, 16.9 mmol) in methanol (25 mL), was added 10% Pd on C (25 mg) and the reaction mixture was stirred under hydrogen atmosphere (balloon) at room temperature. On completion of the reaction as indicated by TLC, the mixture was filtered through a celite pad and the filtrate concentrated to yield the title product 1-Aminomethylcyclopropanecarboxylic acid ethyl esteras a colorless liquid (2.25 g, yield 93%);


1H NMR (DMSO-d6, 300 MHz):
δ 0.8– 0.88 (m, 2H, 2 × CH c-propyl),
1.0–1.07 (m, 2H, 2 × CH c-propyl),
1.16 (t, J = 7.1 Hz, 3H, CH3CH2O-),
2.65 (s, 2H, CH2NH2-methylene),
4.05 (q, J = 7.1 Hz, 2H, CH3CH2O-);



MS (CI): 144.1 (M+1, 100%);



Elemental Analysis found: C, 58.51; H, 9.29; N, 9.64 C7H13NO2 Requires C, 58.72; H, 9.15; N, 9.78.


13C NMR








COSY













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ALIBAG, MAHARASHTRA, INDIA
  1. Alibag - Wikipedia, the free encyclopedia

    en.wikipedia.org/wiki/Alibag
    Alibag (also spelled as Alibaug) is a coastal town and a municipal council in Raigad District in the Konkan region of Maharashtra, India. It is also the ...
    History - ‎Geography - ‎Education - ‎Economy

Map of alibaug

 
 
 



























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