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Showing posts with label Methyl 5-(2. Show all posts
Showing posts with label Methyl 5-(2. Show all posts

Monday 8 August 2016

Methyl 5-(2,2-Dimethoxyethylcarbamoyl)-3-(benzyloxy)-1,4-dihydro-1-(2,2-dimethoxyethyl)-4-oxopyridine-2-carboxylate

Figure


Methyl 5-(2,2-Dimethoxyethylcarbamoyl)-3-(benzyloxy)-1,4-dihydro-1-(2,2-dimethoxyethyl)-4-oxopyridine-2-carboxylate (imp-2)


1H NMR (400 MHz, CDCl3) δ 10.1 (t, J = 5.2 Hz, 1H), 8.4 (s, 1H), 7.3–7.4 (m, 5H), 5.2 (s, 2H), 4.5(t, J = 5.2 Hz, 1H), 4.4 (t, J = 4.4 Hz, 1H), 4.0 (d, J = 4.4hz, 2H), 3.7 (s, 3H), 3.6 (t, J = 6.0 Hz, 2H), 3.4 (s, 6H), 3.3 (s, 6H) ; 
13C NMR (400 MHz, CDCl3) δ 173.2, 164.2, 162.1, 148.2, 144.4, 136.7, 134.8, 128.5, 128.3, 128.1, 119.3, 102.7, 102.4, 74.3, 56.8, 55.6, 53.9, 53.1, 40.8;
 IR (KBr, cm–1): 3201, 3045, 2949, 2835, 1734, 1662, 1610, 1548;
 ESI-MS m/z 479.26.




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SIDON, LEBANON
Map of Sidon Lebanon
Sidon
City in Lebanon
Sidon or Saïda is the third-largest city in Lebanon. It is located in the South Governorate of Lebanon, on the Mediterranean coast, about 40 kilometres north of Tyre and 40 km south of the capital, Beirut. Wikipedia























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