2-(4-methoxy- Phenyl)-N-(8-methyl-phthalazin-1-yl)-acetamide

2-(4-methoxy- Phenyl)-N-(8-methyl-phthalazin-1-yl)-acetamide 

M+H 308; HPLC 1.61 (X); 

¹H NMR (400 MHz, DMSO-d₆) δ [ppm] 10.85 (s, H), 9.68 (s, 1 H), 7.88 - 7.76 (m, 2H), 7.71 (d, J = 7.7 Hz, 1 H), 7.38 - 7.27 (m, 2H), 6.98 - 6.88 (m, 2H), 3.79 (s, 2H), 3.75 (s, 3H), 2.77 (s, 3H);

https://patentscope.wipo.int/search/en/detail.jsf?docId=WO2014206524&recNum=1&maxRec=&office=&prevFilter=&sortOption=&queryString=&tab=PCTDescription

Take a tour
SOLOMON ISLANDS



HONIARA





Malaita, Solomon Islands …









.




.
Gizo, on Ghizo Island, is the capital of the Solomon Islands’ far-flung Western Province, a paradise of coral cays, atolls, lagoons and volcanic islands east of Papua New Guinea where, on a rainy day in late July, crowds flocked to the local netball court for the opening of the inaugural Akuila Talasasa Arts Festival.

Motorised canoes lined up in Gizo Harbour near the daily marketplace.










.









/////////




DRUG APPROVALS BY DR ANTHONY MELVIN CRASTO
http://newdrugapprovals.org/

/////////////

(S)-3-(benzyloxy)-2-methylpropanal

NMR INTERPRETATIONS FOR

(S)-3-(benzyloxy)-2-methylpropanal

VALUES

1H (400 MHz, d Chloroform)

1.15 (3H, d, J 7.0, CH3),

2.63 - 2.72 (1H, m),

3.66 (1H, dd, J 9.5, 5.5),

3.70 (1H, dd, J 9.5, 6.5),

4.54 (2H, s),

7.28-7.39 (5H, m),

9.74 (1H, d, J 1.5) 

13C (101 MHz, d Chloroform)

10.7, 46.8, 70.0, 73.3, 127.6, 127.7, 128.4, 137.8, 203.9.

REFERENCES

Zampella, A.; Sorgente, M.; D'Auria, M. V., Tetrahedron: Asymmetry, 2002, 13, 681 - 685 doi:10.1016/S0957-4166(02)00178-7

Harried, S. S.; Lee, C. P.; Yang, G.;Lee, T. I. H.; Myles, D. C., J. Org. Chem., 2003, 68, 6646 - 6660 doi:10.1021/jo034521r
Omura, K. ; Sharma, A. K.; Swern, D., J. Org. Chem., 1976, 41, 975 - 962 doi:10.1021/jo00868a012

SUPP INFO as entry 7 IN

http://www.rsc.org/suppdata/OB/c0/c0ob00491j/c0ob00491j.pdf

.


 

Take a tour
SOLOMON ISLANDS



HONIARA





Malaita, Solomon Islands …









.




.
Gizo, on Ghizo Island, is the capital of the Solomon Islands’ far-flung Western Province, a paradise of coral cays, atolls, lagoons and volcanic islands east of Papua New Guinea where, on a rainy day in late July, crowds flocked to the local netball court for the opening of the inaugural Akuila Talasasa Arts Festival.

Motorised canoes lined up in Gizo Harbour near the daily marketplace.










.









/////////




DRUG APPROVALS BY DR ANTHONY MELVIN CRASTO
http://newdrugapprovals.org/

/////////