Ethyl 1-Ethyl-4-(4-(N-hydroxycarbamimidoyl)-1-methyl-1H-imidazol-5-yl)-1H-pyrrole-2-carboxylate, 12
hydroxyamidine 12 (58.2 g, 0.191 mol, 89% yield) as off-white plates (mp 226–229 °C):
1H NMR (400 MHz, DMSO-d6) δ 9.15 (s, 1H), 7.67 (s, 1H), 7.50 (d, J = 1.8 Hz, 1H), 7.04 (d, J = 1.8 Hz, 1H), 5.33 (s, 2H), 4.32 (q, J = 7.1 Hz, 2H), 4.23 (q,J = 7.1 Hz, 2H), 1.34 (t, J = 7.1 Hz, 3H), 1.28 (t, J = 7.1 Hz, 3H);
13C NMR (100 MHz, DMSO-d6) δ 160.1, 148.0, 137.2, 130.9, 129.8, 123.8, 120.5, 118.8, 110.5, 59.5, 43.5, 32.2, 16.8, 14.3;
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Qamishli, SYRIA
Al-Qamishli القامشلي Qamişlo |
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City | |
Al-Qamishli
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Location in Syria | |
Coordinates: 37°03′N 41°13′E | |
Country | Syria |
Governorate | Al Hasakah |
District | Al-Qamishli |
Nahiyah | Al-Qamishli |
Founded | 1926 |
Population (2004)Census | |
• Total | 184,231 |
Time zone | EET (UTC+2) |
• Summer (DST) | +3 (UTC) |
Area code(s) | 52 |
The President's street
Al-Qamishli streets during Christmas days
Al-Qamishli Granaries
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