DR ANTHONY MELVIN CRASTO,WorldDrugTracker, helping millions, A 90 % paralysed man in action for you, I am suffering from transverse mylitis and bound to a wheel chair, With death on the horizon, nothing will not stop me except God................DR ANTHONY MELVIN CRASTO Ph.D ( ICT, Mumbai) , INDIA 25Yrs Exp. in the feld of Organic Chemistry,Working for GLENMARK GENERICS at Navi Mumbai, INDIA. Serving chemists around the world. Helping them with websites on Chemistry.Million hits on google, world acclamation from industry, academia, drug authorities for websites, blogs and educational contribution
Showing posts with label 3-(2-methyloxetan-2-yl)pyridine. Show all posts
Showing posts with label 3-(2-methyloxetan-2-yl)pyridine. Show all posts

Sunday, 14 September 2014

3-(2-methyloxetan-2-yl)pyridine



Inline image 3
3-(2-methyloxetan-2-yl)pyridine
Inline image 4
Inline image 5

Inline image 6


Rf 0.28 (Petr. Ether/EtOAc = 20/80). Yellow liquid. 

1H NMR (CDCl3, 399.57 MHz) 
δ 8.63 (d, J = 2.0 Hz, 1H), 
8.50 (dd, J = 4.8, 1.5 Hz, 1H), 
7.80 – 7.67 (m, 1H), 
7.28 (dd, J = 7.9, 4.9 Hz, 1H), 
4.64 (dt, J = 8.6, 6.3 Hz, 1H), 
4.53 (dt, J = 8.7, 6.6 Hz, 1H), 
2.84 (ddd, J = 10.8, 8.7, 7.0 Hz, 1H), 
2.73 (ddd, J = 10.8, 8.8, 6.6 Hz, 1H), 
1.74 (s, 3H). 


13C NMR (CDCl3, 150.92 MHz)
 δ 148.20, 145.89, 
143.17, 131.48, 123.09, 85.06, 64.74, 
35.47, 30.32. 


FTIR (υmax cm-1) 2970, 2883, 1575, 1415, 1289, 1081, 956, 867, 808, 714. 

HRMS Calcd for C9H12NO: 150.0913; Found (M+H) +: 150.0912. 



1H NMR

Inline image 1



13 C NMR


Inline image 2



take a tour
Eritrea, africa


Map of eritrea

Eritrea - Wikipedia, the free encyclopedia

en.wikipedia.org/wiki/Eritrea
Eritrea (/ˌɛrɨˈtreɪ.ə/ or /ˌɛrɨˈtriːə/; Tigrinya: ኤርትራ ʾErtrā ; Arabic: إرتريا‎ ... Its name Eritrea is based on the Greek name for the Red Sea (Ἐρυθρὰ ...

Isaias Afwerki

Isaias Afwerki (sometimes spelled Afewerki; Tigrinya: ኢሳይያስ ...

History of Eritrea

History of Eritrea. Coat of Arms of Eritrea. Pre-colonial. Kingdom ...






asmara















asmara

Massawa Old City



take a tour
Eritrea, africa


Map of eritrea

Eritrea - Wikipedia, the free encyclopedia

en.wikipedia.org/wiki/Eritrea
Eritrea (/ˌɛrɨˈtreɪ.ə/ or /ˌɛrɨˈtriːə/; Tigrinya: ኤርትራ ʾErtrā ; Arabic: إرتريا‎ ... Its name Eritrea is based on the Greek name for the Red Sea (Ἐρυθρὰ ...

Isaias Afwerki

Isaias Afwerki (sometimes spelled Afewerki; Tigrinya: ኢሳይያስ ...

History of Eritrea

History of Eritrea. Coat of Arms of Eritrea. Pre-colonial. Kingdom ...









.





take a tour
Eritrea, africa


Map of eritrea

Eritrea - Wikipedia, the free encyclopedia

en.wikipedia.org/wiki/Eritrea
 
Eritrea (/ˌɛrɨˈtreɪ.ə/ or /ˌɛrɨˈtriːə/; Tigrinya: ኤርትራ ʾErtrā ; Arabic: إرتريا‎ ... Its name Eritrea is based on the Greek name for the Red Sea (Ἐρυθρὰ ...

Isaias Afwerki

Isaias Afwerki (sometimes spelled Afewerki; Tigrinya: ኢሳይያስ ...

History of Eritrea

History of Eritrea. Coat of Arms of Eritrea. Pre-colonial. Kingdom ...






asmara















asmara

Massawa Old City

Eritrea – Island of the Red Seo of Eritrea –
keren



 




 


"Asara" traditional sesami oil press - Eritrea (Saied Ibrahim Yehdego)




 
////////








asmara















asmara

Massawa Old City

Eritrea – Island of the Red Seo of Eritrea –
keren



 




 


"Asara" traditional sesami oil press - Eritrea (Saied Ibrahim Yehdego)




 
////////