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Sunday 14 September 2014

3-(2-methyloxetan-2-yl)pyridine



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3-(2-methyloxetan-2-yl)pyridine
Inline image 4
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Rf 0.28 (Petr. Ether/EtOAc = 20/80). Yellow liquid. 

1H NMR (CDCl3, 399.57 MHz) 
δ 8.63 (d, J = 2.0 Hz, 1H), 
8.50 (dd, J = 4.8, 1.5 Hz, 1H), 
7.80 – 7.67 (m, 1H), 
7.28 (dd, J = 7.9, 4.9 Hz, 1H), 
4.64 (dt, J = 8.6, 6.3 Hz, 1H), 
4.53 (dt, J = 8.7, 6.6 Hz, 1H), 
2.84 (ddd, J = 10.8, 8.7, 7.0 Hz, 1H), 
2.73 (ddd, J = 10.8, 8.8, 6.6 Hz, 1H), 
1.74 (s, 3H). 


13C NMR (CDCl3, 150.92 MHz)
 δ 148.20, 145.89, 
143.17, 131.48, 123.09, 85.06, 64.74, 
35.47, 30.32. 


FTIR (υmax cm-1) 2970, 2883, 1575, 1415, 1289, 1081, 956, 867, 808, 714. 

HRMS Calcd for C9H12NO: 150.0913; Found (M+H) +: 150.0912. 



1H NMR

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13 C NMR


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Eritrea (/ˌɛrɨˈtreɪ.ə/ or /ˌɛrɨˈtriːə/; Tigrinya: ኤርትራ ʾErtrā ; Arabic: إرتريا‎ ... Its name Eritrea is based on the Greek name for the Red Sea (Ἐρυθρὰ ...

Isaias Afwerki

Isaias Afwerki (sometimes spelled Afewerki; Tigrinya: ኢሳይያስ ...

History of Eritrea

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.





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Eritrea, africa


Map of eritrea

Eritrea - Wikipedia, the free encyclopedia

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Eritrea (/ˌɛrɨˈtreɪ.ə/ or /ˌɛrɨˈtriːə/; Tigrinya: ኤርትራ ʾErtrā ; Arabic: إرتريا‎ ... Its name Eritrea is based on the Greek name for the Red Sea (Ἐρυθρὰ ...

Isaias Afwerki

Isaias Afwerki (sometimes spelled Afewerki; Tigrinya: ኢሳይያስ ...

History of Eritrea

History of Eritrea. Coat of Arms of Eritrea. Pre-colonial. Kingdom ...






asmara















asmara

Massawa Old City

Eritrea – Island of the Red Seo of Eritrea –
keren



 




 


"Asara" traditional sesami oil press - Eritrea (Saied Ibrahim Yehdego)




 
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asmara















asmara

Massawa Old City

Eritrea – Island of the Red Seo of Eritrea –
keren



 




 


"Asara" traditional sesami oil press - Eritrea (Saied Ibrahim Yehdego)




 
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