7-Bromo-4-isobutyl-2-methyl-2,6-dihydro-1H-pyrrolo[3,4-d]pyridazin-1-one

Synthesis of 7-Bromo-4-isobutyl-2-methyl-2,6-dihydro-1H-pyrrolo[3,4-d]pyridazin-1-one (6a)

crude oil was purified by flash chromatography (hexane–ethyl acetate, 2:1) to give 6a (0.64 g, 47% yield).

¹H NMR (CDCl₃, 400 MHz) δ 11.59 (br s, 1H), 7.18 (s, 1H), 3.72 (s, 3H), 2.70 (d, J = 7.4 Hz, 2H), 2.12–2.09 (septet, 1H), 0.97 (d, J = 6.6 Hz, 6H).

Domagala, J. M.; Ellsworth, E. L.; Stier, M. A.; Huang, L.; Micetich, R. G.; Singh, R.; Wrigley, S. K.; Wang,S. Warner-Lambert Co. Patent WO9825932A1, 1998; p 48.

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South Sudan, East Africa

South Sudan

Country in East Africa

South Sudan, officially the Republic of South Sudan, is a landlocked country in northeastern Africa that gained its independence from Sudan in 2011. Its current capital is Juba, which is also its largest city. Wikipedia

Capital: Juba

 

 

 

 

 

 

 

  

JUBA

 

 

 

 

 

 

 

 

 

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7-Bromo-4-isobutyl-2-methyl-2,6-dihydro-1H-pyrrolo[3,4-d]pyridazin-1-one

Synthesis of 7-Bromo-4-isobutyl-2-methyl-2,6-dihydro-1H-pyrrolo[3,4-d]pyridazin-1-one (6a)

crude oil was purified by flash chromatography (hexane–ethyl acetate, 2:1) to give 6a (0.64 g, 47% yield).

¹H NMR (CDCl₃, 400 MHz) δ 11.59 (br s, 1H), 7.18 (s, 1H), 3.72 (s, 3H), 2.70 (d, J = 7.4 Hz, 2H), 2.12–2.09 (septet, 1H), 0.97 (d, J = 6.6 Hz, 6H).

Domagala, J. M.; Ellsworth, E. L.; Stier, M. A.; Huang, L.; Micetich, R. G.; Singh, R.; Wrigley, S. K.; Wang,S. Warner-Lambert Co. Patent WO9825932A1, 1998; p 48.

/////////////

South Sudan, East Africa

South Sudan

Country in East Africa

South Sudan, officially the Republic of South Sudan, is a landlocked country in northeastern Africa that gained its independence from Sudan in 2011. Its current capital is Juba, which is also its largest city. Wikipedia

Capital: Juba

 

 

 

 

 

 

 

  

JUBA

 

 

 

 

 

 

 

 

 

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