Experimental double-quantum 14N/1H correlation spectrum of the -NH3 group (I) and the two rigid amide NH pairs (II) in the tripeptide Ala-Ala-Gly. The 2.5 mm rotor was spun at 29.76 kHz in a static field of 18.8 T at 49 °C. (d, f) Experimental cross sections parallel to the vertical dimension of the double-quantum spectrum of sites I and II. (e,g) Simulated double-quantum spectra of sites I and II.
SEE http://smashnmr.org/media/smash/2013/talks/talk_w3.pdf
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