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Showing posts with label MENTHOL. Show all posts
Showing posts with label MENTHOL. Show all posts

Sunday, 23 August 2015

MENTHOL

.

 SPECTRA
 

Sample: menthol
Solvent: CDCl3
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients


Experiment: 2D 1,1-Multiplicity-edited ADEQUATE
Details: AVANCE Tutorial
Pulse program: adeqed11etgpsp
Experiment Time: 4 hours
PARAMETERS
ACQUISITION PROCESSING
2 td=1k
1 td=128w
ns=256
xfb followed by phase correction in both dimensions
2 si=1k
1 si=256w
RELATED ITEMS
 
OBSERVATIONS
Improved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).


 SPECTRA
 

Sample: menthol
Solvent: CDCl3
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients


Experiment: 2D 1,1-Multiplicity-edited refocused-ADEQUATE
Details: AVANCE Tutorial
Pulse program: adeqed11etgprdsp
Experiment Time: 4 hours
PARAMETERS
ACQUISITION PROCESSING
2 td=1k
1 td=128w
ns=256
xfb followed by phase correction in both dimensions
2 si=1k
1 si=256w
RELATED ITEMS
 
OBSERVATIONS
Improved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).



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