DR ANTHONY MELVIN CRASTO,WorldDrugTracker, helping millions, A 90 % paralysed man in action for you, I am suffering from transverse mylitis and bound to a wheel chair, With death on the horizon, nothing will not stop me except God................DR ANTHONY MELVIN CRASTO Ph.D ( ICT, Mumbai) , INDIA 25Yrs Exp. in the feld of Organic Chemistry,Working for GLENMARK GENERICS at Navi Mumbai, INDIA. Serving chemists around the world. Helping them with websites on Chemistry.Million hits on google, world acclamation from industry, academia, drug authorities for websites, blogs and educational contribution

Sunday 23 August 2015

MENTHOL

.

 SPECTRA
 

Sample: menthol
Solvent: CDCl3
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients

Experiment: 2D 1,1-Multiplicity-edited ADEQUATE
Details: AVANCE Tutorial
Pulse program: adeqed11etgpsp
Experiment Time: 4 hours
PARAMETERS
ACQUISITION PROCESSING
2 td=1k
1 td=128w
ns=256		 xfb followed by phase correction in both dimensions
2 si=1k
1 si=256w
RELATED ITEMS
 
OBSERVATIONS
Improved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).


 SPECTRA
 

Sample: menthol
Solvent: CDCl3
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients

Experiment: 2D 1,1-Multiplicity-edited refocused-ADEQUATE
Details: AVANCE Tutorial
Pulse program: adeqed11etgprdsp
Experiment Time: 4 hours
PARAMETERS
ACQUISITION PROCESSING
2 td=1k
1 td=128w
ns=256		 xfb followed by phase correction in both dimensions
2 si=1k
1 si=256w
RELATED ITEMS
 
OBSERVATIONS
Improved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).



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2 comments:

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