N,N-dibutyladamantane-1-carboxamide

Molecular Formula:

	C19H33NO
Molecular Weight:	291.47142 g/mol

N,N - dibutyladamantane - 1 - carboxamide (CAS 116415 - 18 - 0)

White solid (12 mg, 14%).  R f =  0.11 ( 2.5% THF in  petroleum ether ).

1 H NMR (400 MHz, CDCl 3 ):  δ 3.33 (t,  J = 7.9 Hz, 4H), 2.03 (s, 3H), 1.99 (s,  6H),  1.77 – 1.64  (m,  6H) ,  1.56 – 1.43  (m,  4H),  1.38 – 1.19  (m,  4H),  0.94  (t,  J =  7.3  Hz,  6H).

 13 C{ 1 H} NMR (100 MHz, CDCl 3 ): δ 176.4, 47.9, 42.1, 39.4, 36.9, 30.7, 28.8, 20.4, 14.1.

EI - MS:  m/z 291.2

 .G M. Dubowchik, L. Padilla, K. Edinger, R. A. Firestone,J. Org. Chem.1996,61, 4676–4684

1 H NMR (400 MHz, CDCl 3 ):  δ 3.33 (t,  J = 7.9 Hz, 4H), 2.03 (s, 3H), 1.99 (s,  6H),  1.77 – 1.64  (m,  6H) ,  1.56 – 1.43  (m,  4H),  1.38 – 1.19  (m,  4H),  0.94  (t,  J =  7.3  Hz,  6H).

13 C{ 1 H} NMR (100 MHz, CDCl 3 ): δ 176.4, 47.9, 42.1, 39.4, 36.9, 30.7, 28.8, 20.4, 14.1.

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