N,N-dibutyladamantane-1-carboxamide
C19H33NO | |
Molecular Weight: | 291.47142 g/mol |
N,N - dibutyladamantane - 1 - carboxamide (CAS 116415 - 18 - 0)
White solid (12 mg, 14%). R f = 0.11 ( 2.5% THF in petroleum ether ).
1 H NMR (400 MHz, CDCl 3 ): δ 3.33 (t, J = 7.9 Hz, 4H), 2.03 (s, 3H), 1.99 (s, 6H), 1.77 – 1.64 (m, 6H) , 1.56 – 1.43 (m, 4H), 1.38 – 1.19 (m, 4H), 0.94 (t, J = 7.3 Hz, 6H).
13 C{ 1 H} NMR (100 MHz, CDCl 3 ): δ 176.4, 47.9, 42.1, 39.4, 36.9, 30.7, 28.8, 20.4, 14.1.
EI - MS: m/z 291.2
.G M. Dubowchik, L. Padilla, K. Edinger, R. A. Firestone,J. Org. Chem.1996,61, 4676–4684
1 H NMR (400 MHz, CDCl 3 ): δ 3.33 (t, J = 7.9 Hz, 4H), 2.03 (s, 3H), 1.99 (s, 6H), 1.77 – 1.64 (m, 6H) , 1.56 – 1.43 (m, 4H), 1.38 – 1.19 (m, 4H), 0.94 (t, J = 7.3 Hz, 6H).
13 C{ 1 H} NMR (100 MHz, CDCl 3 ): δ 176.4, 47.9, 42.1, 39.4, 36.9, 30.7, 28.8, 20.4, 14.1.
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