1-(2-p-Tolylethynyl)benzene
Compound 3b was prepared according to the general procedure and purified by column chromatography to give a white solid. M.p. 58-60 oC.
1H-NMR (300 MHz, 25 oC, CDCl3, δ ppm): 7.65 – 7.58 (m, 2H), 7.52 (m, 2H), 7.45 – 7.36 (m, 3H), 7.22 (m, 2H), 2.43 (s, 3H); 13C-NMR (75 MHz, 25 oC, CDCl3, δ ppm):138.31, 131.50, 131.46, 129.07, 128.27, 128.02, 123.46, 120.17, 89.56, 88.72, 21.43.
///////////.........

Mom will teach you NMR

///////////////
///////////////
Zhob
City in Pakistan

/////////////
No comments:
Post a Comment