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Monday, 18 July 2016

2-chloro-3-(3-chloro-5-iodophenoxy)-4-(trifluoromethyl)pyridine




2-chloro-3-(3-chloro-5-iodophenoxy)-4-(trifluoromethyl)pyridine


1H NMR (400 MHz, DMSO-d6) δ 8.65 (d, J = 4.9 Hz, 1H), 7.95 (t, J = 4.5 Hz, 1H), 7.60 (dd, J = 1.3, 2.9Hz, 1H), 7.38 (br. s., 1H), 7.29 - 7.15 (m, 1H)


13C NMR (101 MHz, DMSO-d6) δ 157.10, 148.02, 145.37, 142.46 (q, JC-F = 2.0 Hz), 135.00, 132.82 (q,JC-F = 33.2 Hz), 131.69, 122.91, 121.59 (q, JC-F = 4.0 Hz), 121.34 (q, JC-F = 273.7 Hz), 115.47, 95.72

19F NMR (377 MHz, DMSO-d6) δ -61.96 (s, 1F)
mp 71.69-79.27 °C






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