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Saturday 14 June 2014

1-benzoylmorpholine



1-benzoylmorpholine


1H NMR (300 MHz, CDCl3):
7.21-7.40 (m, 5 H, ArH), 
3.50 (br, s, 6H, CH2), ortho to oxygen atom
3.29 (br, s, 2H, CH2 ).  ortho to nitrogen atom


13CNMR (75.5 MHz, CDCl3):
169.8 (CH=O), 134.7 (Ar-Cq), 129.3 (Ar-CH), 128.0 (Ar-CH), 126.5 (Ar-CH), 76.6 (CH2), 74.0 (CH2), 66.3 (CH2).
MS (ESI): m/z 191.0 (M+H)+
Anal. Found (calculated for C10H8N2O): C 69.47 (69.09). H 6.48 (6.85), N 7.02 (7.32)%.


S. Rubino, S. Petruso, R. Pierattelli, G. Bruno, G. C. Stocco, L. Steardo, M. Motta, M. Passerotto, E. Del Giudice and G. Guli, J. Inorg. Biochem., 2004, 98, 2071-2079. http://dx.doi.org/10.1016/j.jinorgbio.2004.09.012
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