2, 3-methoxyphenyl)-N-phthalazin-1-yl-acetamide

 

Synthesis of 2- 3-methoxyphenyl)-N-phthalazin-1-yl-acetamide 

Phthalazin-1-ylamine (57 mg; 0.39 mmol) was suspended in 1 ,2-dichloro-ethane (4 mL) under argon. N-ethyldiisopropylamine (0.141 mL; 0.83 mmol) was added followed by the dropwise addition of (3-methoxyphenyl)-acetyl chloride (0.123 ml; 0.79 mmol) via a syringe. During the addition the temperature increased from 20 °C to 35 °C. After one minute a clear light brown solution was obtained. The reaction was stirred for 18 h at room temperature. The solvent was removed under vacuum. The residue was purified by chromatography (column: 40 g RP18 silica gel; combiflash companion); yield: 6 mg (5 %), colourless solid (purity: 100 %, Rt: 2.94 min); 

¹H NMR (400 MHz, DMSO-d₆) δ [ppm] 10.96 (s, 1H), 9.59 (s, 1 H), 8.19 (d, J = 8.0 Hz, 1 H), 8.08 - 7.79 (m, 3H), 7.29 (t, J = 7.9 Hz, 1 H), 7.10 - 6.74 (m, 3H), 3.86 (s, 2H), 3.77 (s, 3H).

WO2014206524



 GOA FOOD,  INDIA, GOA


 
 KING FISH PICKLE

Mojea Goa Amchi Mumbai

 
 

 

 Mojea Goa Amchi Mumbai
 

 
 Prawns Moile..... Sweet, Sour and Spicy......
 

 Goan Sausages Grays made with Onions and Potatoes n fried with a hint of Vinegar and Coconut Oil severed with Pav....

 Mojea Goa Amchi Mumbai

 

 
Yummy Juicy Mankios...... — with Francisco Xavier Dcosta Goa, Thebigcountryband Goa, Pudhari Goa and 19 others.
 
 
 Mojea Goa Amchi Mumbai

 
 
All set to cook green masala... — with Colin Glen Fernandes, Sarita Uchil Shetty, Alcina Gomes and 15 others.

 
 Mojea Goa Amchi Mumbai

 Mojea Goa Amchi Mumbai

 
 
Posta Fish Rava Fry (King Fish) — with Devyani Toraskar, Aah Goa, Fishermans Wharf Goa and 34 others.
 

 
GÖÄÑ FìSH CÜRRY RìCÉ
 DRY PRAWNS CURRY






 
 
PÖRK CHìLLY FRY. CÜT Ñ CLÉÄÑ PÖRK ìÑ TO MÉDìMìÜM ÖR SMÄLL PìÉCÉS, WÄSH Ñ MÄRìÑÄTÉ WìJH SÄLT ÖR VìÑÉGÄR FÖR MÄX 1 .HÖÜR THÉÑ ìÑ Ä PÅÑ ÖR KÄDÄìL ADD WÅTèR Ñ MÄRìÑATÉD MÉÄT Ñ
LÉT ìT ßÖìL ÖÑCÉ DÖNÉ ÄDD ÖìL Ñ FRY ìT ADD ßìÑDÄ SÖL (KÖKÜM FÜLL) ÖÑìÖÑS, GARLìC Ö GìÑGÉR FìÑÉ CHÖPPÉD, ÖÑìÖÑ, SALT Ñ SAFFRÖÑ POWDÉR Ä PìÑCH ÄÑD GRÉÉÑ CHìLLY SLìT FRY WÉLL Ñ RÉÄDY TÖ SÉRVè... TRY Ñ LÉT MÉ KÑÖW

See Translation

 



/////////////


//////////////////