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Monday, 22 December 2014

N,N-Dimethyl-5-nitropyridin-2-amine



N,N-Dimethyl-5-nitropyridin-2-amine30 (3d)
Yellow solid; mp 155-157 °C; 1H NMR (DMSO-d6, 400 MHz) δ 9.02 (d, 1H, J 2.8 Hz), 8.26 (dd, 1H, J 9.2; 2.8 Hz), 6.80 (d, 1H, J 9.2 Hz), 3.25 (s, 6H); IR (KBr) νmax/cm-1: 2924, 2854, 1597, 1335, 1295, 1118, 810; MS (CI method): 168 (M+1, 100%).
30. Heindel, N. D.; Kannewell, P. D.; Chem. Commun. 1969, 38. 

Journal of the Brazilian Chemical Society

Print version ISSN 0103-5053

J. Braz. Chem. Soc. vol.21 no.8 São Paulo  2010

http://dx.doi.org/10.1590/S0103-50532010000800005

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