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Friday 16 January 2015

L-Kynurenine

L-Kynurenine

Table 1. NMR data for the pheromone in CD3OD/D2O
No.
δC
δH
mult(JHz)
COSY
HMBC
1
174.1




2
52.1
4.01
dd(2.7, 9.0)
H-3, 3'
C-1,3,4
3
40.3
3.55
dd( 9.0,18.5)
H-2, 3'
C-1,2,4
3'

3.75
dd(2.7, 18.5)
H-2, 3
C-1,2,4
4
200.3




5
117.7




6
152.8




7
118.4
6.76
d(8.46)
H-8
C-5
8
136.1
7.27
dd(7.12,8.46)
H-7, 9
C-6
9
116.4
6.62
dd(7.12, 8.08)
H-8, 10

10
132
7.74
d(8.08)
H-9
C-4,5,6
mult, multiplicity; d, doublet; dd, double doublet; COSY, correlation spectroscopy; HMBC, heteronuclear multiple bond correlation.
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