N CHLORO ISATIN

http://www.scielo.br/scielo.php?pid=S0103-50532011000200010&script=sci_arttext

Journal of the Brazilian Chemical Society

Print version ISSN 0103-5053

J. Braz. Chem. Soc. vol.22 no.2 São Paulo Feb. 2011

http://dx.doi.org/10.1590/S0103-50532011000200010 

Spectroscopic data

1a: IR (film) ν _max/cm^-1: 3085, 2923, 1764, 1729, 1614, 1596, 1483, 1315, 1294, 1176, 1126, 950, 427. 

¹H NMRδ (200 MHz, CDCl₃): 3.23 (3H, s), 6.85 (1H, d, J 8.0 Hz), 7.51-7.57 (2H, m); 

¹³C NMR δ (50 MHz, CDCl₃): 26.5 (CH₃), 111.4 (CH), 118.3 (q), 125.2 (CH), 129.7 (q), 137.9 (CH), 149.8 (q), 157.8 (q), 182.4 (q); 

MS (70 eV)m/z 195 [M] ⁺, 197 [M+2] ⁺, 160, 104.