1-benzoylmorpholine

1-benzoylmorpholine

1H NMR (300 MHz, CDCl3):

7.21-7.40 (m, 5 H, ArH), 

3.50 (br, s, 6H, CH2), ortho to oxygen atom

3.29 (br, s, 2H, CH2 ).  ortho to nitrogen atom

13CNMR (75.5 MHz, CDCl3):

169.8 (CH=O), 134.7 (Ar-C_q), 129.3 (Ar-CH), 128.0 (Ar-CH), 126.5 (Ar-CH), 76.6 (CH2), 74.0 (CH2), 66.3 (CH2).

MS (ESI): m/z 191.0 (M+H)+

Anal. Found (calculated for C₁₀H₈N₂O): C 69.47 (69.09). H 6.48 (6.85), N 7.02 (7.32)%.

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S. Rubino, S. Petruso, R. Pierattelli, G. Bruno, G. C. Stocco, L. Steardo, M. Motta, M. Passerotto, E. Del Giudice and G. Guli, J. Inorg. Biochem., 2004, 98, 2071-2079. http://dx.doi.org/10.1016/j.jinorgbio.2004.09.012








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