2,4,6-Tris(2-chloropropan-2-yl)-1,3,5-trioxane

2,4,6-Tris(2-chloropropan-2-yl)-1,3,5-trioxane 


mp 106–108 °C (Lit.(1) 106–107 °C);  

¹H NMR (CDCl₃, 300 MHz) δ = 1.54–1.63 (m, 18 H), 4.86–4.90 (m, 3 H) ppm;  

¹³C NMR (CDCl₃, 75 MHz) δ = 26.7, 67.2, 103.0 ppm;

IR ν_max (solid) 1154, 1122, 1107 cm^–1.

 


ref 1
Stevens, C. L.; Gillis, B. T. J. Am. Chem. Soc. 1957, 79, 3448– 3451, DOI: 10.1021/ja01570a036



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